6 0 obj endstream endobj 56 0 obj <>/Length 9/Matrix[1.0 0.0 0.0 1.0 0.0 0.0]/Resources<>>>/Subtype/Form/Type/XObject>>stream endstream endobj 53 0 obj <>/Length 9/Matrix[1.0 0.0 0.0 1.0 0.0 0.0]/Resources<>>>/Subtype/Form/Type/XObject>>stream 1H and 13C are the most important NMR active nuclei in organic chemistry Natural Abundance 1H 99.9% 13C 1.1% The NMR solvents used to acquire these spectra contain a maximum of 0.05% and 1.0% TMS (v/v) respectively. Appligent StampPDF Batch 4.5.1 3 0 obj 71 0 obj <>/Filter/FlateDecode/ID[]/Index[43 56]/Info 42 0 R/Length 91/Prev 60888/Root 44 0 R/Size 99/Type/XRef/W[1 2 1]>>stream endstream endobj 63 0 obj <>/Subtype/Form/Type/XObject>>stream endstream endobj 60 0 obj <>/Subtype/Form/Type/XObject>>stream endstream endobj 59 0 obj <>/Length 9/Matrix[1.0 0.0 0.0 1.0 0.0 0.0]/Resources<>>>/Subtype/Form/Type/XObject>>stream endstream endobj 51 0 obj <>/Subtype/Form/Type/XObject>>stream endstream endobj 62 0 obj <>/Length 9/Matrix[1.0 0.0 0.0 1.0 0.0 0.0]/Resources<>>>/Subtype/Form/Type/XObject>>stream While single peak solvent suppression is useful for samples where water is the solvent, many organic solvents have multiple strong NMR peaks. endstream endobj 48 0 obj <>/Subtype/Form/Type/XObject>>stream h�b``�b``�e �K�P+�0p��耂$I)(f`x���p��k ���f�!c ��< ),L+�C���܋2�U��020\���n��ff`�="�� �L7�@U���bc`x�"ʨ` !�S /Form Do endstream endobj 50 0 obj <>/Length 9/Matrix[1.0 0.0 0.0 1.0 0.0 0.0]/Resources<>>>/Subtype/Form/Type/XObject>>stream /R0 gs In a proton NMR Spectrum, HOH appears as a singlet. endstream endobj h�bbd``b`�$A�'���@�*�H0I �� �-��*��(o ��"ZA�� ��Q�@��bd82��q���Lw� �� Acrobat Distiller 8.1.0 (Windows); modified using iText 4.2.0 by 1T3XT 2018-01-16T10:43:15-05:00 endobj <>stream In protic solvents, or solvents capable of hydrogen bonding (any compound containing O-H or N-H bonds), the proton attached to the oxygen or nitrogen has some unusual behavior in the NMR spectrum. /MWFOForm Do 98 0 obj <>stream /MWFOForm Do %PDF-1.6 %���� It should be noted that chemical shifts, can be dependent on solvent, concentration and temperature. 1 0 obj endstream endobj 57 0 obj <>/Subtype/Form/Type/XObject>>stream <> endstream endobj 54 0 obj <>/Subtype/Form/Type/XObject>>stream /Form Do endstream endobj 58 0 obj <>>>/ProcSet[/PDF]/XObject<>>>/Subtype/Form/Type/XObject>>stream 0 Issue10.1021/om100106eVoR 43 0 obj <> endobj endobj NMR Chemical Shifts of Trace Impurities: Common Laboratory Solvents, Organics, and Gases in Deuterated Solvents Relevant to the Organometallic Chemist. endstream <> <> endstream endobj startxref /Form Do <> «m» denotes a broad peak with some fine structures. NMR solvent, both the HOH and HOD peaks are observed, but not the DOD.

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